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2) Dried samples are ground to talcum powder consistency (250 um or less) using a ball mill ( Spex Industries 8000) before being sealed into 5 x 9 mm tin capsules. Thorough sample homogenization in the grinder stage is required, to make certain that the tiny subsample taken for analysis ( 24 mg for leaf material) is representative of ...
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• the SPEX 8000 Mixer Mill, shaker type mill with vial clamp speed of 875 cycles per minute; the milling time (0 40 h). The following milling parameters were used: air atmosphere, the ball to power weight ratio was 10:1, the vials and balls were made of stainless steel.
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Spex 8000 Series Mixer / Mill Artisan Technology Group. The SPEX SamplePrep 8000 series Mixer/Mills are efficient, compact laboratory mills capable of pulverizing samples in the 10 gram range. Functionally described as shaker mills or high energy ball mills, these Mixer/Mills shake containers back and forth approximately 1080 cycles per .
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Plant samples must be ovendried, ballmilled to less than 250 um particle size and weighed (~3 mg, with ug digits significant) into 5 x 5 mm tin capsules before combustion. Poor precision can often be traced to inadequate grinding that leaves fibrous matter or visible granules in the sample. Sample prep for totalC/totalN analysis is found below.
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